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- W2783133642 abstract "The effects of exposure to exogenous elements on human health have attracted particular attention. Quantification knowledge of zirconium (Zr) is rather valuable for comprehensive assessments of the biological reactions triggered by a long term presence of the widely used Zr-contained biomedical devices such as prostheses, implants and orthodontic materials. Herein, we reported the first example of the application of cloud point extraction (CPE) couple with inductively coupled plasma mass spectrometry for enrichment and quantification of trace Zr in complex biological samples. The phase separation of CPE was handy without traditional operation like centrifugation and careful pipetting, facilitating high-throughput analysis. Good anti-interference ability against other interference metal ions and outstanding sensitivity with the low detection limit of 0.055 ng·mL−1 were achieved. The satisfactory intra-day and inter-day precisions for low, middle, high concentration levels of Zr were 1.7%–4.2% and 2.0%–6.1%, with the corresponding relative error of 0.1%–7.2% and 0.2%–2.8%, respectively. For practical application, this simple, sensitive and reliable method was applied for enrichment and analysis of trace Zr in rat livers, kidneys and urine. Consequently, trace Zr could be actually detected. Good recoveries of the samples were obtained in the range of 91.0%–118% with the corresponding RSDs (n = 3) of 2.4%–10%." @default.
- W2783133642 created "2018-01-26" @default.
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- W2783133642 date "2018-05-01" @default.
- W2783133642 modified "2023-10-14" @default.
- W2783133642 title "Handy cloud point extraction coupled with inductively coupled plasma mass spectrometry for analysis of trace zirconium in complex biological samples" @default.
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- W2783133642 doi "https://doi.org/10.1016/j.microc.2018.01.013" @default.
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