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- W2783175768 abstract "Abstract We have synthesized InP nanocrystals of an unprecedented crystal phase at low temperature (35–100 °C) by templated growth of InP magic‐sized clusters. With the addition of stoichiometric equivalents of P(SiMe 3 ) 3 to the starting cluster, we demonstrate nanocrystal growth mediated through a partial dissolution and recrystallization pathway. This growth process was monitored using a combination of in situ UV/Vis and 31 P NMR spectroscopy, revealing the intermediacy of smaller cluster species of higher symmetry. The nanocrystals that result from this templated growth exhibit a crystal structure that is neither zincblende nor wurtzite, and instead is derived from the original cluster. This structure is best described as a 3D polytwistane phase as deduced from a combination of X‐ray diffraction, Raman, and solid‐state NMR spectroscopy methods." @default.
- W2783175768 created "2018-01-26" @default.
- W2783175768 creator A5065412580 @default.
- W2783175768 creator A5089168196 @default.
- W2783175768 date "2018-01-24" @default.
- W2783175768 modified "2023-10-17" @default.
- W2783175768 title "Templated Growth of InP Nanocrystals with a Polytwistane Structure" @default.
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- W2783175768 doi "https://doi.org/10.1002/anie.201711539" @default.
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