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• W2783254005 abstract "We report new structural motifs for Cu nanoclusters that conceptually represent seed crystals for large face-centred cubic (FCC) crystal growth. Kinetically controlled syntheses, high resolution mass spectrometry experiments for determination of the dication formulae and crystallographic characterisation were carried out for [Cu18 H16 (DPPE)6 ][BF4 ][Cl] (DPPE=bis(diphenylphosphino)ethane) and [Cu16 H14 (DPPA)6 ][(BF4 )2 ] (DPPA=bis(diphenylphosphino)amine) polyhydrido nanoclusters, which feature the unprecedented bifrustum and frustum metal-core architecture in metal nanoclusters. The Cu18 nanocluster contains two Cu9 frustum cupolae and the Cu16 nanocluster has one Cu9 frustum cupola and a Cu7 distorted hexagonal-shape base. Gas-phase experiments revealed that both Cu18 H16 and Cu16 H14 cores can spontaneously release H2 upon removal of one bisphosphine capping ligand." @default.
• W2783254005 created "2018-01-26" @default.
• W2783254005 creator A5005359088 @default.
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• W2783254005 creator A5077005924 @default.
• W2783254005 creator A5086369378 @default.
• W2783254005 date "2018-01-16" @default.
• W2783254005 modified "2023-10-15" @default.
• W2783254005 title "Synthesis and X‐Ray Crystallographic Characterisation of Frustum‐Shaped Ligated [Cu ₁₈ H ₁₆ (DPPE) ₆ ] ²⁺ and [Cu ₁₆ H ₁₄ (DPPA) ₆ ] ²⁺ Nanoclusters and Studies on Their H ₂ Evolution Reactions" @default.
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• W2783254005 doi "https://doi.org/10.1002/chem.201705448" @default.
• W2783254005 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/29337386" @default.
• W2783254005 hasPublicationYear "2018" @default.
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