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• W2783455522 endingPage "170732" @default.
• W2783455522 startingPage "170732" @default.
• W2783455522 abstract "This paper reports a new route to synthesize calcium carbonate (CaCO 3 )-based nanoscale ionic materials (NIMs) via an in situ formation method to form the CaCO 3 nanoparticles with a polysiloxane quaternary ammonium salt (PQAC) corona (PQAC-CaCO 3 nanoparticles), followed by an ionic exchange reaction to fabricate a poly(ethylene glycol)-tailed sulfonate anion (NPEP) canopy. The chemical compositions and structures of the CaCO 3 -based NIMs synthesized in this work were confirmed by Fourier-transform infrared spectroscopy and solid-state 13 C NMR spectroscopy. Transmission electron microscopic observation indicated that the CaCO 3 -based NIMs presented a rhombohedral shape with a well-defined core-shell structure, and they also obtained an NPEP canopy with a thickness of 4–6 nm. X-ray powder diffraction investigation confirmed that the CaCO 3 inner core had a calcite crystalline structure, whereas the NPEP canopy was amorphous. The NPEP canopy was found to show a characteristic crystallization–melting behaviour in the presence of the ion bonding with PQAC-CaCO 3 nanoparticles according to the characterization of differential scanning calorimetry. Thermogravimetric analysis indicated that the CaCO 3 -based NIMs achieved a high content of NPEP canopy as well as an improvement in thermal stability owing to the ion-bonding effect. Most of all, the CaCO 3 -based NIMs demonstrated a liquid-like behaviour above the critical temperature in the absence of solvent. Moreover, the CaCO 3 -based NIMs also showed a relatively high electrical conductivity with a temperature dependency due to the ionic conductive effect. This work will provide a more feasible and energy-saving methodology for the preparation of CaCO 3 -based NIMs to promote their industrialization and extensive applications." @default.
• W2783455522 created "2018-01-26" @default.
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• W2783455522 date "2018-01-01" @default.
• W2783455522 modified "2023-09-26" @default.
• W2783455522 title "<i>In situ</i> formation of surface-functionalized ionic calcium carbonate nanoparticles with liquid-like behaviours and their electrical properties" @default.
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• W2783455522 doi "https://doi.org/10.1098/rsos.170732" @default.
• W2783455522 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/5792874" @default.
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• W2783455522 hasPublicationYear "2018" @default.
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