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- W2783608630 abstract "Highly condensed nitridosilicates doped with Eu2+ or Ce3+ play an important role in saving energy by converting the blue light of (In,Ga)N-LEDs. Although nitridosilicates are known for great structural variety based on covalent anionic Si-N networks, elemental variety is restricted. Presenting a significant extension of the latter, this work describes a general access to open-shell transition-metal nitridosilicates. As a proof-of-principle, the first iron nitridosilicate, namely Fe2 Si5 N8 , was prepared by exchanging Ca2+ in α-Ca2 Si5 N8 applying a FeCl2 melt (salt metathesis). The title compound was analyzed by powder X-ray diffraction, EDX, ICP-OES, combustion analysis, TG/DSC, Mössbauer spectroscopy and magnetic susceptibility measurements. Furthermore, the structure of α-Ca2 Si5 N8 was determined at 1073 and 1173 K confirming the anionic network of α-Ca2 Si5 N8 providing possible migration pathways for the ion-exchange reaction." @default.
- W2783608630 created "2018-01-26" @default.
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- W2783608630 date "2018-02-05" @default.
- W2783608630 modified "2023-10-03" @default.
- W2783608630 title "Fe2 Si5 N8 : Access to Open-Shell Transition-Metal Nitridosilicates" @default.
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- W2783608630 doi "https://doi.org/10.1002/anie.201713006" @default.
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