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- W2783758940 abstract "The goal of the following procedure is to provide a demonstration of the one-pot conversion of a 2-azido-1-nitrate-ester to a trichloroacetimidate glycosyl donor. Following azido-nitration of a glycal, the product 2-azido-1-nitrate ester can be hydrolyzed under microwave-assisted irradiation. This transformation is usually achieved using strongly nucleophilic reagents and extended reaction times. Microwave irradiation induces hydrolysis, in the absence of reagents, with short reaction times. Following denitration, the intermediate anomeric alcohol is converted, in the same pot, to the corresponding 2-azido-1-trichloroacetimidate." @default.
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- W2783758940 date "2018-01-15" @default.
- W2783758940 modified "2023-09-25" @default.
- W2783758940 title "One-pot Microwave-assisted Conversion of Anomeric Nitrate-esters to Trichloroacetimidates" @default.
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- W2783758940 doi "https://doi.org/10.3791/56610" @default.
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