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- W2784022042 abstract "Ni-free N-containing oxide dispersion strengthened (ODS) austenitic alloys were manufactured by mechanical alloying (MA) followed by spark plasma sintering (SPS). The phase evolutions during milling under a nitrogen atmosphere and after sintering were studied by X-ray diffraction (XRD). Transmission electron microcopy (TEM) and alloy contrast variation analysis (ACV), including small-angle neutron scattering (SANS) and ultra-small-angle X-ray scattering (USAXS), revealed the existence of nanoparticles with a diameter of 3–51 nm for the samples sintered at 950 °C. Sintering at 1000 °C for 5 and 15 min caused slight growth and a significant coarsening of the nanoparticles, up to 70 nm and 128 nm, respectively. The ACV analysis indicated the existence of two populations of Y2O3, ε-martensite and MnO. The dispersive X-ray spectrometry (EDS) confirmed two kinds of nanoparticles, Y2O3 and MnO. The material was characterized by superior micro-hardness, of above 500 HV0.1." @default.
- W2784022042 created "2018-01-26" @default.
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- W2784022042 date "2018-04-01" @default.
- W2784022042 modified "2023-10-18" @default.
- W2784022042 title "Manufacturing and characterization of Ni-free N-containing ODS austenitic alloy" @default.
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- W2784022042 doi "https://doi.org/10.1016/j.jnucmat.2018.01.025" @default.
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