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- W2784265797 abstract "Three types of super paramagnetic core-shell nanoparticles have creatively been synthesized via three basic substances, Fe2+/Fe3+, methacrylic acid (MAA), and 2,2′-azobisisobutyronitrile (AIBN). It has been demonstrated that the order of addition of starting materials determines the type of products. Methacrylic acid coated magnetic nanoparticles (Fe3O4@MAA) with abundant double bonds on the surface, poly methacrylic acid coated magnetic nano particles (Fe3O4@PMAA) having plenty of surface carboxylic groups, and amphiphilic shell of methacrylic acid polymer on magnetic nano particles core (Fe3O4@AMPH) having both carboxyl and alkyl groups on the surface were prepared in three, separate one-pot, sequential synthesis. At first, the resultant magnetic nanoparticles (MNPs) were characterized by transmission electron microscopy (TEM), dynamic light scattering, X-ray spectroscopy, Fourier transform infrared spectroscopy (FTIR) and thermal analysis. Then, the colloidal stability of the synthesized particles was investigated in several common solvents such as water, 1-propanol, chloroform, and edible oil. Finally, the application of each nanoparticle was discussed. It was found that Fe3O4@MAA can be successfully applied as a core in polymerization procedure. Fe3O4@PMAA performed well in nickel uptake and can therefore be used as magnetic solid sorbent in nickel pre-concentration and remediation. Fe3O4@AMPH was well dispersed in oil, suggesting that it can be successfully used as a good extractor in dispersive solid phase pre-concentration and cleanup of both hydrophilic and hydrophobic compounds in heated edible oil samples." @default.
- W2784265797 created "2018-01-26" @default.
- W2784265797 creator A5028261412 @default.
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- W2784265797 date "2018-03-01" @default.
- W2784265797 modified "2023-09-24" @default.
- W2784265797 title "Sequential synthesis of a magnetic nano-adsorbent: How the first step identifies the final product" @default.
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- W2784265797 doi "https://doi.org/10.1016/j.colsurfa.2018.01.004" @default.
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