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- W2785152015 abstract "Simultaneous redox free radical polymerization (FRP) and redox cationic polymerization (CP) are combined for the synthesis of methacrylate/diepoxide interpenetrating polymer networks (IPN). At first, the Cu(acac)2/phosphine/iodonium salt operates according to the principles of free radical promoted cationic polymerization (FRPCP). A photoactivation of the reaction for that system was necessary to enhance the mild methacrylate and diepoxide conversions. Second and at least, two complementary copper catalytic cycles are used simultaneously: the recently developed Cu(II)/reducing agent/peroxide FRP system combined with the older Cu(II)/reducing agent/iodonium salt redox CP system. For this latter hybrid system, outstanding efficiency was observed with more than 90% of epoxy functions conversion for the cationic difunctional monomers and 78% conversion for the vinylic functions conversion for difunctional monomers. The radical and cation generations are discussed in order to fill the interrogations raised by ..." @default.
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- W2785152015 date "2018-01-24" @default.
- W2785152015 modified "2023-10-13" @default.
- W2785152015 title "Copper-Based (Photo)redox Initiating Systems as Highly Efficient Systems for Interpenetrating Polymer Network Preparation" @default.
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- W2785152015 doi "https://doi.org/10.1021/acs.macromol.7b02491" @default.
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