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• W2785348810 startingPage "975" @default.
• W2785348810 abstract "Tethered ruthenium–TsDPEN complexes have been applied to the catalysis of the asymmetric transfer hydrogenation of a range of aryl/acetylenic ketones. The introduction of an ortho- substituent to the aryl ring of the substrate results in a reversal of the enantioselectivity, while the introduction of two o-fluoro substituents results in an improvement to the reduction enantioselectivity, as does the replacement of a phenyl ring on the alkyne with a trimethylsilyl group. These effects are rationalized as resulting from a change in the steric properties of the aryl ring and the electronic properties of the alkyne which, when matched in the reduction transition state, combine within a “window” of substrate/catalyst matching to generate products of high ee." @default.
• W2785348810 created "2018-02-23" @default.
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• W2785348810 date "2018-01-31" @default.
• W2785348810 modified "2023-10-09" @default.
• W2785348810 title "Combining Electronic and Steric Effects To Generate Hindered Propargylic Alcohols in High Enantiomeric Excess" @default.
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• W2785348810 doi "https://doi.org/10.1021/acs.orglett.7b03884" @default.
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