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- W2788004054 abstract "Ir(III)-catalyzed unprecedented mild C–H amidation for weakly coordinating cyclic N-sulfonyl ketimines, accelerated by a mono protected l-amino acid, has been developed. The method uses 1,4,2-dioxazol-5-ones as the robust amidating reagent in conjunction with a catalytic amount of silver triflate. It is highly selective and does not require a stoichiometric amount of oxidants or additives. A series of mechanistic experiments was performed to gain some insights into the reaction mechanism. The strategy provides easy access to novel benzosultam-quinazoline and benzosultam-quinazolinone hybrid scaffolds endowed with pharmaceutically relevant features." @default.
- W2788004054 created "2018-03-06" @default.
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- W2788004054 date "2018-02-23" @default.
- W2788004054 modified "2023-09-26" @default.
- W2788004054 title "Ir(III)/MPAA-Catalyzed Mild and Selective C–H Amidation of <i>N</i>-Sulfonyl Ketimines: Access To Benzosultam-Fused Quinazolines/Quinazolinones" @default.
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- W2788004054 doi "https://doi.org/10.1021/acs.joc.8b00125" @default.
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