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• W2788402920 abstract "Siliceous zeolites are ideally suited for emerging applications in gas separations, sensors, and the next generation of low-k dielectric materials, but the use of fluoride in the synthesis significantly hinders their commercialization. Herein, we show that the dry gel conversion (DGC) technique can overcome this problem. Fluoride-free synthesis of two siliceous zeolites—AMH-4 (CHA-type) and AMH-5 (STT-type), has been achieved for the first time using the method. Siliceous *BEA-, MFI-, and *MRE-type zeolites have also been synthesized to obtain insights into the crystallization process. Charge-balancing interactions between the inorganic cation, organic structure-directing agent (OSDA), and Si−O− defects are found to be an essential aspect. We quantify this factor in terms of the “OSDA charge/silica ratio” of the as-made zeolites and demonstrate that the DGC technique is broadly applicable and opens up new avenues for fluoride-free siliceous zeolite synthesis." @default.
• W2788402920 created "2018-03-06" @default.
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• W2788402920 date "2018-02-21" @default.
• W2788402920 modified "2023-09-27" @default.
• W2788402920 title "Broadening the Scope for Fluoride‐Free Synthesis of Siliceous Zeolites" @default.
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• W2788402920 doi "https://doi.org/10.1002/anie.201712684" @default.
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