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- W2788671305 abstract "This paper presents a facile, rapid, and controllable procedure for the recovery of trace Ag+ ions and in situ assembly of well dispersed Ag nanoparticles on chitosan-TiO2 composites through bioaffinity adsorption followed by photocatalytic reduction. The prepared Ag nanoparticles are proven to be efficient and recyclable nanocatalysts for the reduction of 4-nitrophenol to 4-aminophenol in the presence of NaBH4. Well dispersed quasi-spherical Ag NPs are synthesized in 20 min in the designed inner-irradiated photocatalytic system under a wide range of Ag+ concentrations (50–200 mg l−1), temperatures (10 °C–25 °C) conditions, and UV or visible light irradiation. The synthesized Ag NPs can catalyze the reduction of 4-nitrophenol by NaBH4 at 100% conversion in 120 min and preserve the catalytic activity in five successive cycles. This procedure for trace Ag+ ions recovery and Ag NPs assembly has the potential to be scaled up for the mass production of recyclable Ag nanocatalysts. The present work provides a green and efficient procedure for the conversion of hazardous 4-nitrophenol to industrially important 4-aminophenol and also sheds a light on designing scaled-up procedures for treating high volumes of wastewater with dilute heavy metals to produce recyclable metallic nanocatalysts in aqueous systems." @default.
- W2788671305 created "2018-03-06" @default.
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- W2788671305 date "2018-02-20" @default.
- W2788671305 modified "2023-10-18" @default.
- W2788671305 title "Facile synthesis of dispersed Ag nanoparticles on chitosan-TiO<sub>2</sub> composites as recyclable nanocatalysts for 4-nitrophenol reduction" @default.
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- W2788671305 doi "https://doi.org/10.1088/1361-6528/aaac74" @default.
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