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• W2789110003 endingPage "391" @default.
• W2789110003 startingPage "385" @default.
• W2789110003 abstract "A poly(vinylidene fluoride-co-hexafluoropropylene)-based polymer inclusion membrane (PIM) using Cyphos® IL 101 (i.e. trihexyl(tetradecyl)phosphonium chloride) as the carrier and 2-nitrophenyl octyl ether as a plasticizer in a mass ratio of 55/35/10 was employed for the on-line extractive separation of V(V) prior to its spectrophotometric determination in a flow injection analysis (FIA) system using xylenol orange as the colorimetric reagent. The selectivity of the membrane allowed the determination of V(V) in sulfate solutions in the presence of a variety of cations and anions. The interference of molybdenum(VI) was eliminated by off-line extraction using the same PIM. A univariate sequential optimization of the newly developed FIA system was conducted and under optimal conditions the system is characterized by a linear concentration range of 0.5–8.0 mg L−1, detection limit of 0.08 mg L−1 and sample throughput of 4 h−1. The relative standard deviation at the 3 mg L−1 level of V(V) was 2.9% based on 8 replicate determinations. The membrane was stable, which was reflected by the standard deviation value for determinations over three consecutive days (24 determinations of 3 mg L−1 V(V)) of 3.6%. The newly developed FIA system was applied to the determination of V(V) in water and dietary supplements samples and a good agreement with inductively coupled plasma optical emission spectrometry was observed." @default.
• W2789110003 created "2018-03-06" @default.
• W2789110003 creator A5046310353 @default.
• W2789110003 creator A5047465931 @default.
• W2789110003 creator A5047770644 @default.
• W2789110003 creator A5086010507 @default.
• W2789110003 date "2018-05-01" @default.
• W2789110003 modified "2023-10-14" @default.
• W2789110003 title "Flow injection spectrophotometric determination of V(V) involving on-line separation using a poly(vinylidene fluoride-co-hexafluoropropylene)-based polymer inclusion membrane" @default.
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• W2789110003 doi "https://doi.org/10.1016/j.talanta.2018.01.042" @default.
• W2789110003 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/29426530" @default.
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