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• W2789808467 abstract "An atomic absorption spectrometer unit fitted with a graphite furnace module is used to perform high temperature treatment on three carbonized polymers: polyvinyl chloride (PVC), polyvinylidene chloride (PVDC) and polyacrylonitrile (PAN). Using short pulses up to 45 s, we heat small samples to a maximum of 3000 °C. High-resolution transmission electron microscopy and X-ray diffractometry are used to track the growth of crystallites in the materials as a function of the heating temperature. We observe the well-known behaviour of large crystalline graphite growth in PVC-derived samples and the formation of curved graphitic layers in PVDC- and PAN-derived samples. This graphite furnace atomic absorption spectrometer approach is an attractive alternative to conventional laboratory-scale graphite furnaces in research of high temperature treatment of carbon and other refractory materials." @default.
• W2789808467 created "2018-03-29" @default.
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• W2789808467 date "2018-08-01" @default.
• W2789808467 modified "2023-10-18" @default.
• W2789808467 title "Pulsed thermal treatment of carbon up to 3000 °C using an atomic absorption spectrometer" @default.
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• W2789808467 doi "https://doi.org/10.1016/j.carbon.2018.03.060" @default.
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