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• W2789984070 abstract "Abstract A new family of three P,P-diphenylphosphinic amide-TEMPO radicals with general formula (C6H5)2P(X)-NH-TEMPO, X = O (1), S (2) and Se (3) were obtained by reaction of chlorodiphenylphosphine with 4-amino-2,2,6,6-tetramethylpiperidine-1-oxyl radical (NH2-TEMPO) and subsequent oxidation with H2O2 and elemental sulfur or selenium. These radicals were characterized by UV–Vis, FT-IR and 1H, 31P and 77Se nuclear magnetic resonance spectroscopy. The crystal structures of all radicals were determined by single-crystal X-ray diffraction. The magnetic study of all diphenylphosphinic amide-TEMPO radicals reveals very weak intermolecular ferromagnetic interactions. Density functional theory (DFT) calculations have been also performed to support the interpretation of magnetic properties and electronic structure." @default.
• W2789984070 created "2018-03-29" @default.
• W2789984070 creator A5004507012 @default.
• W2789984070 creator A5006117834 @default.
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• W2789984070 creator A5070426822 @default.
• W2789984070 creator A5074417930 @default.
• W2789984070 creator A5089898620 @default.
• W2789984070 date "2018-04-01" @default.
• W2789984070 modified "2023-09-27" @default.
• W2789984070 title "Novel P,P-diphenylphosphinic amide-TEMPO radicals family: Synthesis, crystal structures, spectroscopic characterization, magnetic properties and DFT calculations" @default.
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