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• W2790033956 abstract "The catalytic asymmetric methylation of fluoroalkylated pyruvates is shown with dimethylzinc as a methylating reagent in the presence of a copper catalyst bearing a chiral phosphine ligand. This is the first catalytic asymmetric methylation to synthesize various α-fluoroalkylated tertiary alcohols with CF 3 , CF 2 H, CF 2 Br, and n -C n F 2 n +1 ( n = 2, 3, 8) groups in good-to-high yields and enantioselectivities. Axial backbones and substituents on phosphorus atoms of chiral phosphine ligands critically influence the enantioselectivity. Moreover, the methylation of simple perfluoroalkylated ketones is found to be facilitated by only chiral phosphines without copper." @default.
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• W2790033956 date "2018-03-07" @default.
• W2790033956 modified "2023-10-16" @default.
• W2790033956 title "Copper-catalyzed asymmetric methylation of fluoroalkylated pyruvates with dimethylzinc" @default.
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• W2790033956 doi "https://doi.org/10.3762/bjoc.14.44" @default.
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