Matches in SemOpenAlex for { <https://semopenalex.org/work/W2790252382> ?p ?o ?g. }
- W2790252382 abstract "An efficient aqueous sodium dichloroiodate ( $$hbox {NaICl}_{2})$$ mediated protocol is developed for the synthesis of benzofused azoles by the cyclization of 2-amino anilines/thiophenols/phenols with $$beta $$ -diketone compounds. The reactions gave moderate to good yield of the corresponding 2-substituted benzimidazoles/benzothiazoles/benzoxazoles under mild conditions. This tandem process involved a C-C bond cleavage and C-N bond formation. SYNOPSIS A facile and single protocol for the synthesis of three versatile 1,3-benzazoles viz 2-substituted 1H-benzimidazoles, benzoxazoles and benzothiazoles from readily available starting materials, 1,3-diketones and corresponding o-amino anilines/thiophenols/phenols, by aqueous sodium dichloroiodate ( $$hbox {NaICl}_{2})$$ mediated C—C bond cleavage has been developed. The reaction provides a rapid access to these 1, 3-benzazoles in good yields, thus speeding up the drug discovery process." @default.
- W2790252382 created "2018-03-29" @default.
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- W2790252382 date "2018-01-01" @default.
- W2790252382 modified "2023-09-26" @default.
- W2790252382 title "Sodium dichloroiodate promoted C-C bond cleavage: An efficient synthesis of 1,3-Benzazoles via condensation of $${varvec{o}}$$ o -amino/mercaptan/hydroxyanilines with $${varvec{beta }}$$ β -diketones" @default.
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- W2790252382 doi "https://doi.org/10.1007/s12039-017-1414-z" @default.
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