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- W2790674863 abstract "The synthesis of a 6,6'-ester linked disaccharide analog model compound was achieved in five steps from d-glucose and featured a key oxidative esterification transformation. The synthesized d-gluco-pyranosyl-(6,6')-d-gluco-pyranuronate was characterized in D2O using NMR spectroscopy. Using the experimental data together with molecular dynamics simulations (TIP3P, water), a model of the compound's conformational behavior was established. The effect of the 6,6'-ester linkage on the solution phase structure was compared to that of the previously reported 6,6'-ether linkage in a disaccharide analog. Based on the established models, the ester linkage was found to have a profound effect on the overall shape of the molecule." @default.
- W2790674863 created "2018-03-29" @default.
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- W2790674863 date "2018-03-01" @default.
- W2790674863 modified "2023-10-17" @default.
- W2790674863 title "Synthesis and conformational analysis of d-gluco-pyranosyl-(6,6′)-d-gluco-pyranuronate, a model compound for the inter-glycan 6,6′-ester linkage" @default.
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- W2790674863 doi "https://doi.org/10.1016/j.carres.2018.01.005" @default.
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