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• W2790896684 abstract "Single electron transfer (SET)-triggered radical ion-based reactions have proven to be powerful options in synthetic organic chemistry. Although unique chain processes have been proposed in various photo- and electrochemical radical ion-based transformations, the turnover number, also referred to as catalytic efficiency, remains unclear in most cases. Herein, we disclose our investigations of radical cation chain processes in the electrocatalytic Diels-Alder reaction, leading to a scalable synthesis. A gram-scale synthesis was achieved with high current efficiency of up to 8000%. The reaction monitoring profiles showed sigmoidal curves with induction periods, suggesting the involvement of intermediate(s) in the rate determining step." @default.
• W2790896684 created "2018-03-29" @default.
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• W2790896684 date "2018-03-16" @default.
• W2790896684 modified "2023-10-09" @default.
• W2790896684 title "Investigating radical cation chain processes in the electrocatalytic Diels–Alder reaction" @default.
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• W2790896684 doi "https://doi.org/10.3762/bjoc.14.51" @default.
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