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- W2791128610 abstract "Abstract [(CH2)7(NH3)2]CoCl4 crystallizes in the triclinic system, space group P-1 with two molecules per asymmetric unit cell (Z = 2). The unit cell dimensions are a = 7.3107 (2) A, b = 10.1841 (3) A, c = 11.2690 (4) A, α = 66.81 (2), β = 78.85 (12), and γ = 87.66 (2). The unit cell volume and the calculated density are 756.11 (4) A3 and 1.463 Mg m−3, respectively. The structure of the hybrid is characterized by alternating layers of inorganic [CoCl4]2– anion and heptane diammonium cation. The organic hydrocarbon layers are packed in a stacked herring-bone manner with hydrogen bonds to the halide ions. The lattice potential energy Upot and the cation molecular volume V+ are 1856.2 kJ/mol and 0.37 nm3, respectively. DSC showed a compound (broad) peak at T1 = 331 K, T2 = 328 K with total entropy ΔS = 36.2 J/K. mol, and a λ-like endothermic peak at T3 = 296 K (ΔS = 24.9 J/K. mol). Dielectric properties are investigated at different temperatures and frequencies [260 K" @default.
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- W2791128610 date "2018-07-01" @default.
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- W2791128610 title "Structure, thermal, and impedance study of a new organic–inorganic hybrid [(CH 2 ) 7 (NH 3 ) 2 ]CoCl 4" @default.
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- W2791128610 doi "https://doi.org/10.1016/j.jpcs.2018.02.048" @default.
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