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• W2793378033 abstract "Abstract To improve the quality of industrial nitrile rubbers, the copolymer chemical composition, p A ( t ), should ideally be kept constant along the reaction. This work proposes a closed‐loop control strategy for the semibatch operation of the reactor with the aim of regulating p A ( t ) within a reduced range of variability. The proposed strategy is evaluated by simulating a mathematical model of the process. To this effect, a simplified mathematical model of the reaction is first derived and then utilized to obtain a suboptimal control law and a soft‐sensor that estimates the polymerization rates. The suboptimal control law is compensated by adding a term proportional to errors in p A ( t ). The simulated example considers the production of the low‐composition AJLT grade, with the copolymerization reaction represented by a detailed mathematical model adjusted to an industrial plant. Due to the high performance of the soft‐sensor, the simulation results suggest that the proposed closed‐loop strategy is efficient to adequately regulate p A ( t ) in spite of structural and parametric uncertainties, while other quality variables remained practically unaffected." @default.
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• W2793378033 date "2018-01-18" @default.
• W2793378033 modified "2023-10-16" @default.
• W2793378033 title "A Closed-Loop Control Strategy for Producing Nitrile Rubber of Uniform Chemical Composition in a Semibatch Reactor: A Simulation Study" @default.
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• W2793378033 doi "https://doi.org/10.1002/mren.201700054" @default.
• W2793378033 hasPublicationYear "2018" @default.
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