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• W2795424098 abstract "The electrochemical behavior of Ti(III) ions in a eutectic KF–KCl molten salt was investigated using cyclic voltammetry, square wave voltammetry, and chronoamperometry at 923 K. Ti(III) ions were produced by the addition of 0.50 mol% of K2TiF6 and 0.33 mol% of Ti sponge to the melt. The reduction of Ti(III) ions to metallic Ti was observed as a single 3-electron wave around 0.33 V vs. K+/K in the square-wave voltammogram. The electrodeposition was conducted at a Mo electrode by galvanostatic electrolysis at −50 mA cm−2 for 20 min. The deposits were confirmed to be compact and adherent Ti metal films by scanning electron microscopy, energy dispersive X-ray analysis and X-ray diffraction analysis. The oxidation of Ti(III) to Ti(IV) was observed at 1.82 V vs. K+/K as a reversible electrochemical process. The diffusion coefficient of Ti(III) ions was determined to be 3.9 × 10−5 cm2 s−1." @default.
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• W2795424098 date "2018-01-01" @default.
• W2795424098 modified "2023-10-01" @default.
• W2795424098 title "Electrochemical Behavior of Ti(III) Ions in a KF–KCl Eutectic Melt" @default.
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• W2795424098 doi "https://doi.org/10.5796/electrochemistry.17-00082" @default.
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