FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2796166704> ?p ?o ?g. }

• W2796166704 endingPage "51" @default.
• W2796166704 startingPage "41" @default.
• W2796166704 abstract "A novel extraction technique is proposed in which the Multiple Headspace Extraction (MHE) approach is used in conjunction with Headspace Sorptive Extraction (HSSE) and Gas Chromatography-Mass Spectrometry (GC-MS) detection. The extraction method was developed to determine volatile compounds in macroalgae. Optimization of the extraction parameters was carried out using design of experiments to identify factors that affect the extraction: extraction time, temperature, twister length and amount of sample. The results of the optimization led to an extraction of 2 g of sample using a 20 mm Twister® at 66 °C for 180 min. The progression constants (β) were calculated for 43 volatile compounds, 29 of which could be quantified using the method. Linearity was attained with a determination coefficient higher than 0.99 for all studied compounds. Inter-day and inter-twister precisions ranged from 0.22% to 19.01% and from 0.69% to 14.76% respectively, and values below 10% were obtained for the majority of compounds. LOD and LOQ values ranged from the values obtained for diethyl succinate (0.012 μg/L and 0.088 μg/L, respectively) and those obtained for dimethyl sulfide (5.544 μg/L and 40.286 μg/L, respectively). However, for the majority of compounds values obtained were below 1 μg/L (LOD) and 5 μg/L (LOQ). Compounds such as ethyl acetate, hexanal, heptadecane, 2-hexenal, 6-methyl-5-hepten-2-one, dimethyl sulfide, benzyl alcohol, beta ionone, or beta cyclocitral, among others were correctly determined in three species of macroalgae: Ulva sp., Gracillaria sp. and Enteromorpha sp." @default.
• W2796166704 created "2018-04-13" @default.
• W2796166704 creator A5067061126 @default.
• W2796166704 creator A5089131860 @default.
• W2796166704 creator A5090684514 @default.
• W2796166704 date "2018-05-01" @default.
• W2796166704 modified "2023-09-25" @default.
• W2796166704 title "Optimization of a multiple headspace sorptive extraction method coupled to gas chromatography-mass spectrometry for the determination of volatile compounds in macroalgae" @default.
• W2796166704 cites W1608593301 @default.
• W2796166704 cites W1972266735 @default.
• W2796166704 cites W1981018219 @default.
• W2796166704 cites W1989012697 @default.
• W2796166704 cites W1993195578 @default.
• W2796166704 cites W1999447763 @default.
• W2796166704 cites W2000938893 @default.
• W2796166704 cites W2001421007 @default.
• W2796166704 cites W2008871681 @default.
• W2796166704 cites W2009066188 @default.
• W2796166704 cites W2013919440 @default.
• W2796166704 cites W2028616806 @default.
• W2796166704 cites W2031304400 @default.
• W2796166704 cites W2036260300 @default.
• W2796166704 cites W2037752106 @default.
• W2796166704 cites W2041525884 @default.
• W2796166704 cites W2044870089 @default.
• W2796166704 cites W2047265937 @default.
• W2796166704 cites W2047793019 @default.
• W2796166704 cites W2059268665 @default.
• W2796166704 cites W2065134627 @default.
• W2796166704 cites W2070137827 @default.
• W2796166704 cites W2075887322 @default.
• W2796166704 cites W2076775694 @default.
• W2796166704 cites W2077351891 @default.
• W2796166704 cites W2078409772 @default.
• W2796166704 cites W2084458242 @default.
• W2796166704 cites W2090213159 @default.
• W2796166704 cites W2097259216 @default.
• W2796166704 cites W2102650353 @default.
• W2796166704 cites W2118314854 @default.
• W2796166704 cites W2135157097 @default.
• W2796166704 cites W2146531482 @default.
• W2796166704 cites W2217350064 @default.
• W2796166704 cites W2337670344 @default.
• W2796166704 cites W2549856950 @default.
• W2796166704 cites W2567421240 @default.
• W2796166704 cites W2740938926 @default.
• W2796166704 cites W776211248 @default.
• W2796166704 doi "https://doi.org/10.1016/j.chroma.2018.04.011" @default.
• W2796166704 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/29650482" @default.
• W2796166704 hasPublicationYear "2018" @default.
• W2796166704 type Work @default.
• W2796166704 sameAs 2796166704 @default.
• W2796166704 citedByCount "25" @default.
• W2796166704 countsByYear W27961667042019 @default.
• W2796166704 countsByYear W27961667042020 @default.
• W2796166704 countsByYear W27961667042021 @default.
• W2796166704 countsByYear W27961667042022 @default.
• W2796166704 countsByYear W27961667042023 @default.
• W2796166704 crossrefType "journal-article" @default.
• W2796166704 hasAuthorship W2796166704A5067061126 @default.
• W2796166704 hasAuthorship W2796166704A5089131860 @default.
• W2796166704 hasAuthorship W2796166704A5090684514 @default.
• W2796166704 hasConcept C123460561 @default.
• W2796166704 hasConcept C162356407 @default.
• W2796166704 hasConcept C178790620 @default.
• W2796166704 hasConcept C185592680 @default.
• W2796166704 hasConcept C205345274 @default.
• W2796166704 hasConcept C2778353584 @default.
• W2796166704 hasConcept C2778413813 @default.
• W2796166704 hasConcept C2779440274 @default.
• W2796166704 hasConcept C43617362 @default.
• W2796166704 hasConcept C4725764 @default.
• W2796166704 hasConcept C518881349 @default.
• W2796166704 hasConceptScore W2796166704C123460561 @default.
• W2796166704 hasConceptScore W2796166704C162356407 @default.
• W2796166704 hasConceptScore W2796166704C178790620 @default.
• W2796166704 hasConceptScore W2796166704C185592680 @default.
• W2796166704 hasConceptScore W2796166704C205345274 @default.
• W2796166704 hasConceptScore W2796166704C2778353584 @default.
• W2796166704 hasConceptScore W2796166704C2778413813 @default.
• W2796166704 hasConceptScore W2796166704C2779440274 @default.
• W2796166704 hasConceptScore W2796166704C43617362 @default.
• W2796166704 hasConceptScore W2796166704C4725764 @default.
• W2796166704 hasConceptScore W2796166704C518881349 @default.
• W2796166704 hasLocation W27961667041 @default.
• W2796166704 hasLocation W27961667042 @default.
• W2796166704 hasOpenAccess W2796166704 @default.
• W2796166704 hasPrimaryLocation W27961667041 @default.
• W2796166704 hasRelatedWork W1991134895 @default.
• W2796166704 hasRelatedWork W2007757232 @default.
• W2796166704 hasRelatedWork W2029378756 @default.
• W2796166704 hasRelatedWork W2033413454 @default.
• W2796166704 hasRelatedWork W2051188305 @default.
• W2796166704 hasRelatedWork W2081925920 @default.
• W2796166704 hasRelatedWork W2096652817 @default.
• W2796166704 hasRelatedWork W2118349567 @default.
• W2796166704 hasRelatedWork W2412300609 @default.
• W2796166704 hasRelatedWork W2796166704 @default.

• next