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- W2797341802 abstract "ABSTRACTUltrahigh-performance liquid chromatography coupled with evaporative light scattering detector was used to optimize acid hydrolysis conditions of polysaccharides from Dendrobium candidum. The optimized conditions were the concentration of H2SO4, 0.4 M, hydrolysis temperature, 90°C, and hydrolysis time, 1 h. Ultrahigh-performance liquid chromatography-quadrupole time-of-flight mass spectrometry was used to obtain the total ion current chromatograms and determine the hydrolyzates of polysaccharides, such as monosaccharides, oligosaccharides, and some low-molecular weight polysaccharides from D. candidum, Cordyceps sinensis, and Ganoderma atrum. The accurate mass data were analyzed by chemometric tools, including an unsupervised analytical method, principal component analysis (one-way ANOVA, p < 0.05), and five supervised analytical methods, partial least square discriminant analysis, support vector machine, naive Bayes, decision tree, and neural network. The results showed that D. candidum polysacch..." @default.
- W2797341802 created "2018-04-24" @default.
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- W2797341802 date "2018-04-09" @default.
- W2797341802 modified "2023-09-26" @default.
- W2797341802 title "Determination of Polysaccharide Hydrolyzates in Chinese Herbal Medicine by UltraHigh-Performance Liquid Chromatography-Quadrupole Time-of-Flight Mass Spectrometry and Evaporative Light Scattering Detection" @default.
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- W2797341802 doi "https://doi.org/10.1080/00032719.2017.1396337" @default.
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