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• W2797923003 abstract "The synthesis of an appropriately functionalized advanced C(6–28) fragment (3) of the marine macrolide iriomoteolide-2a (1) has been achieved in a highly efficient manner. The C(6)–C(18) fragment of 1 is prepared via a radical cyclization of a vinyl ether intermediate and palladium-promoted hydrostannylation/iodination. Paterson aldol reaction and Peterson olefination are used to construct the C(19)–C(28) fragment. The union of the C(6)–C(18) and C(19)–C(28) fragments is accomplished via a Suzuki–Miyaura coupling reaction." @default.
• W2797923003 created "2018-04-24" @default.
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• W2797923003 date "2018-04-10" @default.
• W2797923003 modified "2023-10-16" @default.
• W2797923003 title "Studies toward the Synthesis of Iriomoteolide-2a: Construction of the C(6)–C(28) Fragment" @default.
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• W2797923003 doi "https://doi.org/10.1021/acs.orglett.8b00542" @default.
• W2797923003 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/29633846" @default.
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