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- W2799871778 abstract "Abstract An aqueous biphasic system based on cholinium propanoate and phosphate solution was developed for the fast extraction and determination of bisphenol A in honey samples. The phase diagrams of the aqueous biphasic systems with cholinium propanoate (ionic liquid) and phosphate solutions were investigated, and the biphasic regions of the aqueous biphasic systems decreased with the increase of pH values of the phosphate solutions. The aqueous biphasic system was applied for the analyte extraction. After extraction, the analyte was separated on a C 18 column (150 mm × 2.1 mm i. d., 5 μm) using acetonitrile and ammonium acetate as the mobile phase. The parameters, such as the conductivity and viscosity of the ionic liquid solutions, pH values of the phosphate solutions, and extraction efficiency were optimized to achieve the excellent extraction performance. Good linearity was shown for the analyte over the tested concentration range (0.01–10.0 mg/kg) with correlation coefficient higher than 0.991. Three spiked levels (0.01, 0.05, 0.10 mg/kg) were applied for determination of the recoveries of the analyte in honey samples in the range of 78–112% with relative standard deviations of 5.5–10.2%. The limit of detection and limit of quantification for the analyte were 0.003 and 0.01 mg/kg, respectively. The developed method was applied for the determination of the analyte in real samples with high sensitivity." @default.
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- W2799871778 date "2018-05-01" @default.
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- W2799871778 title "Extraction of bisphenol A in honey samples using aqueous biphasic systems coupled with high-performance liquid chromatography" @default.
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- W2799871778 doi "https://doi.org/10.1002/sscp.201800019" @default.
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