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• W2800490912 abstract "Initially unsaturated material frozen with prefabricated porosity was prepared to experimentally investigate its effect on freeze‐drying of liquid material. Ceftriaxone sodium, a kind of commonly used antibiotic, was selected as the primary solute in an aqueous solution. The liquid nitrogen ice cream‐making method was employed to prepare frozen materials with different initial porosities. Results showed that freeze‐drying was significantly enhanced with the initially unsaturated frozen material and substantial drying time was saved compared with conventional freeze‐drying. Drying time for the unsaturated sample (0.3 of saturation or 0.67 of initial porosity) was more than 20 % shorter than that required for the saturated one (1.0 of saturation without initial porosity). SEM images displayed that the dried products of the unsaturated frozen material had a pierced solid skeleton and uniform pore space with a fine and tenuous structure compared with those of the saturated one. The freezing rate exhibited little influence on the freeze‐drying process. Annealing can be moderately beneficial to shortening the drying time and further improving the energy utilization. An appropriate increase in operating temperature was able to enhance the freeze‐drying rate while changes in chamber pressure had a negligible effect on the process." @default.
• W2800490912 created "2018-05-17" @default.
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• W2800490912 date "2018-05-18" @default.
• W2800490912 modified "2023-09-25" @default.
• W2800490912 title "Freeze-drying of ceftriaxone sodium solution frozen with prefabricated porosity" @default.
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• W2800490912 doi "https://doi.org/10.1002/cjce.23232" @default.
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