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- W2800536940 abstract "A simple, straightforward, for the peptide bond formation employing corresponding carboxylic acids and amines derived from amino acids via Nα-protected diacyldiselenide is delineated. The key step of the synthesis is the in situ generation of Nα-protected diacyldiselenide using NaBH2Se3 as selenating reagent, followed by trapping with an amino acid ester leading to the peptide. The formation of Nα-protected diacyldiselenide was confirmed through TLC and HRMS analysis using crude sample. The reaction is clean and all the products were obtained in moderate to good yields, including for sterically hindered amino acids. The protocol is free from racemisation, compatible with Fmoc, Cbz and Boc groups." @default.
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- W2800536940 date "2018-04-21" @default.
- W2800536940 modified "2023-09-23" @default.
- W2800536940 title "Peptide Bond Formation via Nα-Protected Diacyldiselenides" @default.
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- W2800536940 doi "https://doi.org/10.1007/s10989-018-9711-z" @default.
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