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• W2802736712 endingPage "4878" @default.
• W2802736712 startingPage "4873" @default.
• W2802736712 abstract "The first ruthenium-catalyzed umpolung carboxylation of hydrazones with CO2 to generate important aryl acetic acids is reported. Besides aldehyde hydrazones, a variety of ketone hydrazones, which have not been successfully applied in previous umpolung reactions with other reactive electrophiles, also show high reactivity and selectivity under mild conditions. Moreover, this operationally simple protocol features good functional group tolerance, is readily scalable, and offers easy derivation of important structures, including bioactive felbinac and adiphenine. Computational studies reveal that this umpolung reaction proceeds through the generation of a Ru-nitrenoid followed by concerted [4 + 2] cycloaddition with CO2." @default.
• W2802736712 created "2018-05-17" @default.
• W2802736712 creator A5012093734 @default.
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• W2802736712 date "2018-01-01" @default.
• W2802736712 modified "2023-10-17" @default.
• W2802736712 title "Ruthenium-catalyzed umpolung carboxylation of hydrazones with CO₂" @default.
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