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- W2803074971 abstract "In this work, the authors intentionally employ the oxalic acid (OA) to replace terephthalic acid to synthesise a novel zirconium oxalate under the similar reaction condition with UIO-66. The powder X-ray diffraction and thermal gravimetric analysis confirm that as-synthesised zirconium oxalate is a pure phase and oxalate serves as bridging ligand. Scanning electron microscope indicates that zirconium oxalate is aggregated together by several micrometres of needle-like crystals. After zirconium oxalate is calcined at 500°C, the product is the pure tetragonal zirconia (ZrO 2) with high crystallinity. The morphology and particle size of ZrO 2 are basically unmodified with a comparison with the zirconium oxalate. X-ray photoelectron spectroscopy reveals that the structural carbon acts as a phase transformation promoter to stabilise the tetragonal ZrO 2." @default.
- W2803074971 created "2018-05-17" @default.
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- W2803074971 date "2018-07-01" @default.
- W2803074971 modified "2023-10-14" @default.
- W2803074971 title "t ‐ZrO 2 prepared by a novel zirconium oxalate synthesised solvothermally" @default.
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- W2803074971 doi "https://doi.org/10.1049/mnl.2017.0711" @default.
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