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• W2803297156 abstract "Two novel binuclear lanthanide complexes, [Ln(3-Cl-4-MOBA)3(5,5′‐DM‐2,2′‐bipy)]2(5,5′‐DM‐2,2′‐bipy) (Ln = Eu(1), Gd(2)), 3-Cl-4-MOBA = 3-chloro-4-methoxybenzoate; 5,5′‐DM‐2,2′‐bipy = 5,5′-dimethy-2,2′-bipyridine) have been successfully synthesized under hydrothermal conditions. The complexes are characterized by single-crystal X-ray diffraction and elemental analysis. Complexes 1 and 2 are isomorphous, and each metal center is eight-coordinated with a distorted square-antiprism coordination geometry. The binuclear units are assembled into 1D, 2D and 3D supramolecular structures by weak hydrogen bonds (CH···O and CH···Cl) and π–π stacking interactions. Thermal behavior of the complexes 1 and 2 was determined by TG/DSC-FTIR techniques. Heat capacities of the complexes are measured by a DSC instrument in the temperature range of 283.15–393.15 K. Based on the heat capacities date, the thermodynamic functions (HT-H298.15K) and (ST-S298.15K) were obtained. The activation energy E values of the first decomposition stage for complexes 1 and 2 were calculated by integral iso-conversional nonlinear (NL-INT) method. The fluorescence spectra and lifetime of complex 1 (Eu3+ ion) were studied in depth." @default.
• W2803297156 created "2018-06-01" @default.
• W2803297156 creator A5016518424 @default.
• W2803297156 creator A5023172582 @default.
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• W2803297156 date "2019-05-01" @default.
• W2803297156 modified "2023-09-26" @default.
• W2803297156 title "Crystal structure, thermochemical and fluorescent properties of two novel binuclear lanthanide complexes with 3-chloro-4-methoxybenzoic acid and 5,5′-dimethy-2,2′-bipyridine" @default.
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• W2803297156 doi "https://doi.org/10.1016/j.jct.2018.05.020" @default.
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