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- W2803656871 abstract "Abstract We report the synthesis and detailed characterization of amorphous carbon globules containing Fe/Fe3C-graphite core–shell type nanoparticles. The samples were synthesized via a low-cost chemical vapour deposition (CVD) method by the single-step pyrolysis of precursors (benzene and ferrocene). The amount of precursors and the reaction temperature were found to control the morphology of the carbon globules, and the shape, size, composition and distribution of Fe/Fe–C based nanoparticles inside the carbon globules. At the CVD tube wall deposition of Fe derived from the decomposed-ferrocene forms Fe3C particles at high temperature, which are unstable in carbon rich environment and transforms to γ -Fe and carbon-product (graphite). Furthermore, γ -Fe is also unstable at RT and transforms to α -Fe and Fe3C phases while cooling. A fraction of γ -Fe is, however, kinetically arrested during the cooling process. This leads to the formation of ‘Fe/Fe3C (core)-graphite (shell)’ nanoparticles-embedded amorphous carbon globules." @default.
- W2803656871 created "2018-06-01" @default.
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- W2803656871 date "2018-10-01" @default.
- W2803656871 modified "2023-09-29" @default.
- W2803656871 title "One-step pyrolytic synthesis and growth mechanism of core–shell type Fe/Fe<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML id=mml11 display=inline overflow=scroll altimg=si11.gif><mml:msub><mml:mrow /><mml:mrow><mml:mn>3</mml:mn></mml:mrow></mml:msub></mml:math>C-graphite nanoparticles-embedded carbon globules" @default.
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- W2803656871 doi "https://doi.org/10.1016/j.nanoso.2018.05.005" @default.
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