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• W2804249185 abstract "Reaction between pyrogallol and benzaldehyde results in a conformational mixture of C-tetra(phenyl)pyrogallol[4]arene (crown and chair). The conformer mixture was separated using crystallization procedures and the structures were determined using FTIR, 1H-NMR, and 13C-NMR. O-acetylation of C-tetra(phenyl)pyrogallol[4]arene (chair) with acetic anhydride, in pyridine results in the formation of dodecaacetyl-tetra(phenyl)pyrogallol[4]arene. The structure was determined using 1H-NMR and 13C-NMR finding that the product maintains the conformation of the starting conformer. On the other hand, the O-acetylation reaction of C-tetra(phenyl)pirogallol[4]arene (crown) under same conditions proceeded efficiently, and its structure was determined using 1H-NMR and 13C-NMR. Dynamic 1H-NMR of acetylated pyrogallolarene was studied by means of variable temperature in DMSO-d6 solution, and it revealed that two conformers are formed in the solution. Boat conformations for acetylated pyrogallolarene showed a slow interconversion at room temperature." @default.
• W2804249185 created "2018-06-01" @default.
• W2804249185 creator A5047884638 @default.
• W2804249185 creator A5081220866 @default.
• W2804249185 date "2018-05-20" @default.
• W2804249185 modified "2023-09-25" @default.
• W2804249185 title "Conformational Aspects of the O-acetylation of C-tetra(phenyl)calixpyrogallol[4]arene" @default.
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• W2804249185 doi "https://doi.org/10.3390/molecules23051225" @default.
• W2804249185 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/6100403" @default.
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