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• W2804635591 abstract "A series of P-E-containing heterocycles (E=chalcogen) with aromatic backbones were synthesised and characterised by single-crystal and powder XRD, microanalysis and mass spectrometry. Solution- and solid-state 31 P and 77 Se NMR spectroscopy revealed significant differences between the NMR parameters in solution and in the solid state, related to conformational changes in the molecules. Many compounds were shown to exhibit a number of different polymorphic structures (identified by single-crystal XRD), although the bulk material studied by solid-state NMR spectroscopy often contained just one major polymorph. For the unoxidised heterocycles, the presence of weak intermolecular J couplings was also investigated by DFT calculations." @default.
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• W2804635591 date "2018-06-28" @default.
• W2804635591 modified "2023-10-17" @default.
• W2804635591 title "Polymorphism, Weak Interactions and Phase Transitions in Chalcogen-Phosphorus Heterocycles" @default.
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• W2804635591 doi "https://doi.org/10.1002/chem.201800978" @default.
• W2804635591 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/6099295" @default.
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