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- W2805536306 abstract "A borate-containing caged triarylphosphine L-X (X = Na or NBu4), featuring a 9-phospha-10-boratriptycene framework, was synthesized and characterized by NMR spectroscopy and X-ray diffraction analysis. The NMR coupling constant of the corresponding phosphine selenide indicated a higher electron-donating property of the borate-phosphine L compared to that of the 9-phospha-10-silatriptycene derivative (Ph-TRIP). The coordination property of L-X to [PdCl(η3-allyl)]2 was dependent on the countercation, giving a neutral Pd complex [PdCl(η3-allyl)(L-NBu4)] from L-NBu4 in CH2Cl2 or a zwitterionic Pd complex [Pd(η3-allyl)(MeCN)(L)] from L-Na in MeCN/CH2Cl2. Utility of L-X as a ligand for metal catalysis was demonstrated in the Pd-catalyzed Suzuki–Miyaura cross-coupling of aryl chlorides." @default.
- W2805536306 created "2018-06-13" @default.
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- W2805536306 date "2018-06-07" @default.
- W2805536306 modified "2023-09-24" @default.
- W2805536306 title "Synthesis, Properties, and Catalytic Application of a Triptycene-Type Borate-Phosphine Ligand" @default.
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- W2805536306 doi "https://doi.org/10.1021/acs.organomet.8b00113" @default.
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