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• W2806080166 endingPage "9832" @default.
• W2806080166 startingPage "9828" @default.
• W2806080166 abstract "Abstract The large number and structural beauty of silicates are largely due to the variety of connection mode of SiO 4 tetrahedra. SiO 6 and SiF 6 octahedra are also known and give rise for structural versatility of inorganic silicates. However, to date, the crystal structure of inorganic fluorooxosilicates with oxofluoride SiO x F 4− x or SiO x F 6− x species are unknown. Now, fluorine was successfully introduced into the silicophosphates, and the first fluorooxosilicophosphate K 4 Si 3 P 2 O 7 F 12 with an unprecedented SiO 2 F 4 species was synthesized. The existence of Si−F bonds was verified by comprehensively experimental and theoretical work. Using ab initio and bond valence calculations, the oxofluoride SiO x F 6− x species is shown to be stable when oxygen atoms connect to other atoms with strong covalent interactions. This work will contribute to the structural diversity of silicate chemistry by the exploration of the new fluorooxosilicates." @default.
• W2806080166 created "2018-06-13" @default.
• W2806080166 creator A5011991695 @default.
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• W2806080166 creator A5090456026 @default.
• W2806080166 date "2018-07-03" @default.
• W2806080166 modified "2023-10-18" @default.
• W2806080166 title "A Fluorooxosilicophosphate with an Unprecedented SiO₂F₄ Species" @default.
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• W2806080166 doi "https://doi.org/10.1002/anie.201805759" @default.
• W2806080166 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/29869824" @default.
• W2806080166 hasPublicationYear "2018" @default.
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