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- W2806357539 abstract "The trichloroacetimidate group is one of the most versatile leaving groups in organic synthesis. This is evident by its involvement in quite a number of total syntheses. Typical methods of preparation generally involve the use of toxic and hazardous solvents, specifically dichloromethane and chloroform. Liquified Dimethyl ether (DME), was investigated as an alternative solvent in the synthesis of commonly utilized trichloroacetimidates. A range of alcohol substrates were employed and moderate to excellent yields of the corresponding imidates were obtained. The low boiling point (−24 °C) of DME allows for rapid evaporation at atmospheric pressure, and its facile recovery." @default.
- W2806357539 created "2018-06-13" @default.
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- W2806357539 date "2018-09-01" @default.
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- W2806357539 title "Liquefied dimethyl ether (DME) as a green solvent in chemical reactions: Synthesis of O -alkyl trichloroacetimidates" @default.
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- W2806357539 doi "https://doi.org/10.1016/j.scp.2018.06.001" @default.
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