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- W2807183930 abstract "Abstract The assigned structure of the dinoflagellate‐derived toxin belizentrin was prepared by total synthesis in form of the corresponding methyl ester for stability reasons. The successful route features an unusual solution for the preparation of a recalcitrant ylide on a C‐glycosidic segment; moreover, it involves an asymmetric hetero‐Diels–Alder reaction en route to the tertiary hemiacetal substructure, a Negishi cross‐coupling of two elaborate building blocks, and a macrocyclization based on an intramolecular aminolysis of a spirolactone. A modified Kocienski olefination ultimately allowed the polyol side chain to be attached to the macrocycle although this transformation faced the exceptional base sensitivity of this polyunsaturated target compound." @default.
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- W2807183930 date "2018-06-26" @default.
- W2807183930 modified "2023-10-14" @default.
- W2807183930 title "Total Synthesis of Belizentrin Methyl Ester: Report on a Likely Conquest" @default.
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- W2807183930 doi "https://doi.org/10.1002/anie.201805125" @default.
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