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- W2807975959 abstract "The γ-irradiation of a biphasic system composed of tri-n-butylphosphate in tetrapropylene hydrogen (TPH) in contact with palladium(ii) nitrate in nitric acid aqueous solution led to the formation of two precipitates. A thorough characterization of these solids was performed by means of various analytical techniques including X-Ray Diffraction (XRD), Thermal Gravimetric Analysis coupled with a Differential Scanning Calorimeter (TGA-DSC), X-ray Photoelectron Spectroscopy (XPS), InfraRed (IR), RAMAN and Nuclear Magnetic Resonance (NMR) Spectroscopy, and ElectroSpray Ionization Mass Spectrometry (ESI-MS). Investigations showed that the two precipitates exhibit quite similar structures. They are composed at least of two compounds: palladium cyanide and palladium species containing ammonium, phosphorous or carbonyl groups. Several mechanisms are proposed to explain the formation of Pd(CN)2." @default.
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- W2807975959 date "2018-01-01" @default.
- W2807975959 modified "2023-10-09" @default.
- W2807975959 title "Characterization of palladium species after γ-irradiation of a TBP–alkane–Pd(NO<sub>3</sub>)<sub>2</sub>system" @default.
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- W2807975959 doi "https://doi.org/10.1039/c8ra02695e" @default.
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