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- W2810583645 abstract "Surface-enhanced infrared absorption spectroscopy is used in situ to determine the electrochemical stability of organic interfaces deposited onto the surface of nanostructured, thin-film gold electrodes via the electrochemical reduction of diazonium salts. These interfaces are shown to exhibit a wide electrochemical stability window in both acetonitrile and phosphate buffer, far surpassing the stability window of thiol-derived self-assembled monolayers. Using the same in situ technique, the application of radical scavengers during the electrochemical reduction of diazonium salts is shown to moderate interface formation. Consequently, the heterogeneous charge-transfer resistance can be reduced sufficiently to enhance the direct electron transfer between an immobilized redox-active enzyme and the electrode. This was demonstrated for the oxygen-tolerant [NiFe] hydrogenase from the “Knallgas” bacterium Ralstonia eutropha by relating its electrochemical activity for hydrogen oxidation to the interface properties." @default.
- W2810583645 created "2018-07-10" @default.
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- W2810583645 date "2018-06-26" @default.
- W2810583645 modified "2023-10-17" @default.
- W2810583645 title "In Situ Spectroelectrochemical Studies into the Formation and Stability of Robust Diazonium-Derived Interfaces on Gold Electrodes for the Immobilization of an Oxygen-Tolerant Hydrogenase" @default.
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- W2810583645 doi "https://doi.org/10.1021/acsami.8b02273" @default.
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