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- W2819252008 abstract "The analysis experiment methods of fracturing fluid were many and varied, but microstructure analysis of fracturing fluid had not appropriate experimental method. Fracturing fluid sample was feasible after sample preparation including high-pressure freezing, vacuum freezing transport, freeze break etching, sublimation, ion sputtering spraying in turn, which could be observed under high vacuum. Using scanning electron microscopy (SEM) analysis with high vacuum conditions, different kinds of fracturing fluid microstructure in three basic conditions were studied. The experimental results showed that fracturing fluid had liquid, gel, and gel breaking liquid three base states with preparing, cross-linking, and breaking three processes, the corresponding microstructure changes from line to net to linear–net mixed structure. Fracturing fluid types, the concentration of thickener, and other factors directly affected the microstructure of fracturing fluid: Gel had different network structure and network density. Gel with low concentration thickener had low viscosity, bad gel hang, easy gel breaking, and gel corresponding microstructure was more sparse; experiment observed surfactant fracturing fluid’s micelles were linear structure and had layer-linear mixed existence state. Microstructure studied establish the connection between fracturing fluid microstructure and macro-performance to provide experimental methods and evidence for analysis and improving fracturing fluid formula." @default.
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- W2819252008 date "2018-07-12" @default.
- W2819252008 modified "2023-09-22" @default.
- W2819252008 title "Analysis of Fracturing Fluid Microstructure by Scanning Electron Microscope" @default.
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- W2819252008 doi "https://doi.org/10.1007/978-981-10-7560-5_81" @default.
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