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Matches in SemOpenAlex for { <https://semopenalex.org/work/W2820143441> ?p ?o ?g. }

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• W2820143441 abstract "An allylic cis-epoxide prepared by Sharpless asymmetric epoxidation was transformed in nine steps and 41% overall yield to the cyclization precursor 4 via a key one carbon homologation. Cobalt-catalyzed aerobic oxidative cyclization of 4 gave the trans-THF in 94% yield at gram scale. Subsequent manipulations, including a Still–Gennari olefination, Sharpless asymmetric dihydroxylation, Corey–Fuchs alkynylation, and Kazmaier hydrostannylation provided the fully functionalized C(1)–C(9) fragment 2 suitable for cross-coupling. The sequence is readily scalable and provides gram quantities of 2." @default.
• W2820143441 created "2018-07-19" @default.
• W2820143441 creator A5002433378 @default.
• W2820143441 creator A5053915881 @default.
• W2820143441 date "2013-10-01" @default.
• W2820143441 modified "2023-10-03" @default.
• W2820143441 title "Gram scale synthesis of the C(1)–C(9) fragment of amphidinolide C" @default.
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• W2820143441 doi "https://doi.org/10.1016/j.tet.2013.07.026" @default.
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