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- W285515100 abstract "A selective glycosylation strategy enabling access to all stereochemical combinations of tumor associated Thomsen-nouveau (Tn) antigen, d-GalNAc-O-Ser/Thr, has been developed. The key component for selectivity is the phthalimide-protected d- or l-amino acid acceptors which allow access to α- or β-anomers in excellent yields (72–96%) and selectivity (∼100%) when appropriate C-2 substitution is installed. The glycoamino acid intermediates were divergently converted to Tn-based carboxylates or to hydrazides by tandem Pd–C debenzylation followed by treatment with hydrazine hydrate or hydrazine hydrate treatment alone." @default.
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- W285515100 date "2015-05-19" @default.
- W285515100 modified "2023-09-27" @default.
- W285515100 title "Stereoselective Synthesis of Natural and Non-natural Thomsen-nouveau Antigens and Hydrazide Derivatives" @default.
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- W285515100 doi "https://doi.org/10.1021/acs.orglett.5b00512" @default.
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