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- W2864915797 abstract "Abstract Ring-opening polymerization of α-amino acid N- carboxyanhydrides (NCAs) is a powerful synthetic methodology for generating well-defined functional polypeptides. However, conventional procedures require a compromise between obtaining controlled microstructures and employing the optimized polymerization conditions. Specifically, a versatile method to access sequenced cyclic polypeptides remains challenging due to the difficulty in site-specific cyclization. Here we describe a general and straightforward method for the synthesis of both linear and cyclic polypeptides using organocatalytic living polymerization of NCAs. The use of an air-stable organocatalyst, imidazolium hydrogen carbonate, allows for the rapid and controlled polymerization of a variety of NCAs, leading to high conversion within a few minutes under mild conditions. Linear and cyclic block copolypeptides are also accessible simply by controlling the type of initiators and the order of addition of NCA monomers." @default.
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- W2864915797 date "2018-07-18" @default.
- W2864915797 modified "2023-10-16" @default.
- W2864915797 title "Straightforward access to linear and cyclic polypeptides" @default.
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- W2864915797 doi "https://doi.org/10.1038/s42004-018-0040-0" @default.
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