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- W2883039689 abstract "The mesoporous silicoaluminophosphate SAPO-11 materials were synthesized by using the green and low-cost sucrose as template. The SAPO-11 were characterized by SEM, TEM, N2 physisorption and FT-IR. Sucrose was incorporated into the crystal structure of SAPO-11 crystals to form secondary mesoporosity. Meanwhile, the mesoporous MoVI/SAPO-11 samples with different MoO3 crystalline phases were synthesized. In addition, the pre-prepared optimal catalyst (with 3.6% molybdenum mass content) showed significantly high yield and durability for oxidative desulfurization (ODS). Interestingly, the yield of α-MoO3 composites was more than twice that of pure mesoporous SAPO-11 samples, due to the synergistic effect of secondary mesoporosity and molybdenum oxide. Then, the ODS reaction products were determined by GC-MS and 1H NMR. The leaching of active species in the liquid under the reaction conditions were evaluated. Besides, the kinetic properties were studied to calculate the activation energy of the reaction, and then a plausible mechanism of oxidative desulphurization reaction was also proposed." @default.
- W2883039689 created "2018-08-03" @default.
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- W2883039689 date "2018-12-01" @default.
- W2883039689 modified "2023-10-16" @default.
- W2883039689 title "Sucrose facilitated synthesis of mesoporous silicoaluminophosphate SAPO-11 with different crystalline phases of MoO3 for highly-efficient oxidative desulfurization" @default.
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- W2883039689 doi "https://doi.org/10.1016/j.jcis.2018.07.074" @default.
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