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- W2883148462 abstract "The copper zinc tin sulfide (CZTS) compound is a promising candidate as an alternative absorber material for thin-film solar cells. In this study, we investigate the direct formation of $mathrm{C}{mathrm{u}}_{1.92}mathrm{ZnS}{mathrm{n}}_{x}(mathrm{S}{mathrm{b}}_{1ensuremath{-}x}){mathrm{S}}_{4}$ compounds $text{[CZT}(A)text{S]}$, with $x=1$, 0.85, 0.70, and 0.50, via a mechanochemical synthesis (MCS) approach, starting from powders of the corresponding metals, zinc sulfide, and sulfur. The thermal stability of the $text{CZT}(A)text{S}$ compounds was evaluated in detail by in situ synchrotron high-energy x-ray diffraction measurements up to 700 ifmmode^circelsetextdegreefi{}C. The $text{CZT}(A)text{S}$ compounds prepared via MCS revealed a sphalerite-type crystal structure with strong structural stability over the studied temperature range. The contribution of the MCS to the formation of such a structure at room temperature is analyzed in detail. Additionally, this study provides insights into the MCS of CZTS-based compounds: the possibility of a large-scale substitution of Sn by Sb and the production of single phase $text{CZT}(A)text{S}$ with a Cu-poor/Zn-poor composition. A slight increase in the band gap from 1.45 to 1.49--1.51 eV was observed with the incorporation of Sb, indicating that these novel compounds can be further explored for thin-film solar cells." @default.
- W2883148462 created "2018-08-03" @default.
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- W2883148462 date "2018-07-24" @default.
- W2883148462 modified "2023-10-18" @default.
- W2883148462 title "Investigation of single phase Cu2ZnSnxSb1−xS4 compounds processed by mechanochemical synthesis" @default.
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- W2883148462 doi "https://doi.org/10.1103/physrevmaterials.2.075404" @default.
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