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- W2883238229 abstract "Methyl 2-methoxy-5-aminosulfonyl benzoate as an intermediate of sulpiride was synthesized from salicylic acid as precursor, which generally consisted of four reactive steps as to etherification, sulfonyl chloride, amine and lipid. Here in, after optimization of reaction conditions such as molar ratio, reaction time and reaction temperature, the yield of the four-step reactions can be improved as to 92.6% (etherification), 95.7% (sulfonyl chloride), 75.8% (amine) and 97.4%(esterification), respectively, which resulted to the efficient improvement of total yield (63.7%). The structures and purity of all synthesized compounds was confirmed by 1HNMR and HPLC." @default.
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- W2883238229 date "2018-07-01" @default.
- W2883238229 modified "2023-10-14" @default.
- W2883238229 title "Process Optimization of Methyl 2-Methoxy-5-Aminosulfonyl Benzoate" @default.
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- W2883238229 doi "https://doi.org/10.1088/1757-899x/382/2/022064" @default.
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