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• W2884005498 abstract "Solvothermal reaction of Zn(NO3)2·6H2O with 1,4-bis(2-(pyridin-4-yl)vinyl)benzene (1,4-bpeb) and 1,3,5-benzenetricarboxylic acid (1,3,5-H3BTC) (molar ratio = 1:1:3) at 120 °C in CH3CN/H2O (v/v = 1:2) produced a one-dimensional (1D) coordination polymer {[1,4-bpebH2][Zn(H2O)(1,3,5-HBTC)(μ-1,3,5-HBTC)]·2H2O}n (1; [1,4-bpebH2]2+ = 4,4′-(-1,4-phenylenebis(ethene-2,1-diyl))bis(pyridin-1-ium)) in 64% yield. Heating 1 at 160 °C for 5 h gave rise to another 1D coordination polymer {[1,4-bpebH2][Zn(1,3,5-HBTC)(η,η,η,-μ3-1,3,5-HBTC)]·1.5H2O}n (2) in a quantitative yield. Compounds 1 and 2 were characterized by elemental analysis, IR spectroscopy, thermogravimetric analysis, powder X-ray diffraction, and single-crystal X-ray diffraction. Compound 1 consists of [Zn(H2O)(1,3,5-HBTC)] units which are interlinked by μ-1,3,5-HBTC2− ligands to form a 1D [Zn(H2O)(1,3,5-H2BTC)(μ-1,3,5-HBTC)]n2n– anionic chain with [1,4-bpebH2]2+ cations located in-between these chains. Compound 2 contains [Zn2(1,3,5-HBTC)2] units which are interconnected to yield a 1D ladder-type [Zn(1,3,5-HBTC)(η,η,η-μ3-1,3,5-HBTC)]n2n– with [1,4-bpebH2]2+ cations positioned in-between these chains. Upon heating, the anionic single chain structure of 1 undergoes a single-crystal-to-single-crystal topological transformation into the anionic ladder-shaped chain structure of 2 by replacing the coordinated water molecules in one chain via one μ-1,3,5-HBTC2− ligand in the other chain in 1. Both compounds exhibit excellent sorption performance towards Congo Red (CR) in water at room temperature with the maximum absorption capacity of 2020 mg g−1 (1) or 2320 mg g−1 (2). Compound 1 as a representative example can selectively absorb CR from its combination with selected cationic dyes in water." @default.
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• W2884005498 date "2018-11-01" @default.
• W2884005498 modified "2023-10-17" @default.
• W2884005498 title "A Zn(II)-based 1D coordination polymer: Temperature-induced SCSC transformation and selective sorption of Congo Red" @default.
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• W2884005498 doi "https://doi.org/10.1016/j.poly.2018.07.031" @default.
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