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• W2884184564 startingPage "10551" @default.
• W2884184564 abstract "Resonance ionization mass spectrometry (RIMS) combines tunable laser spectroscopy with mass spectrometry to provide a high-efficiency means of analyzing solid materials. We previously showed a very high useful yield of 24% for analysis of uranium using three lasers to excite and ionize atoms sputtered from metallic uranium and uranium dioxide. A new resonance ionization scheme using only two lasers achieves a higher useful yield of 38% by accessing both the ground electronic state and a low-lying electronic state of atomic uranium that is significantly populated by sputtering. The major loss channel in analyzing uranium dioxide is the formation of UOx molecules during sputtering. Prebombardment of the surface with 3 keV noble gas ions prior to analysis reduces the surface and results in a sputtered flux with a greatly enhanced proportion of atomic U. This method of surface reduction results in uranium useful yields as high as 6.6% for uranium dioxide analysis, compared to 2% from previous work." @default.
• W2884184564 created "2018-08-03" @default.
• W2884184564 creator A5021527362 @default.
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• W2884184564 creator A5059114745 @default.
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• W2884184564 date "2018-07-21" @default.
• W2884184564 modified "2023-10-14" @default.
• W2884184564 title "New Resonance Ionization Mass Spectrometry Scheme for Improved Uranium Analysis" @default.
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• W2884184564 doi "https://doi.org/10.1021/acs.analchem.8b02656" @default.
• W2884184564 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30032601" @default.
• W2884184564 hasPublicationYear "2018" @default.
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